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For more information, contact David Eppstein by email at
deppstein@masco.harvard.edu, or by calling 617-632-2860.

Guidelines for the Preparation of a Request for Proposals for an In-Situ Pilot-Scale Feasibility Study of Mercury Removal Technology

 

 1.0 Introduction

This Request for Proposals (RFP) describes the requirements of an in situ pilot-scale feasibility study (FS) of an industrial wastewater treatment (IWWT) system specifically designed for mercury removal. The requirements for completing this FS are described more completely in the following sections, but the following summary is provided to introduce potentially interested vendors to this project.

The Massachusetts Water Resources Authority (MWRA) presently has an enforcement limit of 0.001 milligram (mg) per liter (L) or 1.0 parts per billion (ppb) for mercury discharged by permitted users to the MWRA collection system. This standard has proven to be difficult to achieve for many MWRA customers even when using aggressive pollution prevention methods coupled with traditional end-of-pipe IWWT systems. Therefore, pilot testing of mercury-removal IWWT systems is being requested by a consortium to investigate mercury removal technologies that have the potential to meet the stringent MWRA requirements.

The successful bidder (Vendor) will be required to provide all necessary IWWT equipment components, appurtenances, interconnections, resources and labor as may be required to install the equipment on-site, establish its performance as "steady state" over a period of two to three weeks, then operate the equipment for a period of not less than two (2) consecutive processing weeks (14 straight days) to demonstrate its ability to lower effluent mercury concentrations to minimum levels. The vendor will also be required to conduct sampling and analysis, as described below, necessary to obtain information on serial process operation removal efficiency under load. Following completion of the pilot testing, the vendor will be required to remove the equipment and restore the area to its original condition. The vendor will then be required to prepare a report summarizing field conditions and results obtained, interpret the analytical results of the testing, identifying any operational and maintenance difficulties encountered, and provide a detailed estimate of scale-up costs for the full-system design inclusive of design parameters, sustained system performance and costs (capital, installation and operating). A proposed report outline is presented in Section 4.0.

2.0 Wastewater Characterization / Design Basis

The mercury content of the wastewater produced by the facility undergoing pilot-testing will vary depending upon whether the facility includes clinical laboratories, research laboratories, incinerators and/or laundry facilities. Extensive studies have been conducted to help quantify the mercury concentrations present in wastewater streams discharged from each of these specific hospital facilities. A summary of the mercury data is presented in Table 1. A more complete summary of mercury and other pollutant parameters known to be present is presented in Table 2.

Table 1: Total Mercury Concentration in Typical Wastewater by Area

Area Minimum(ug/L) Maximum(ug/L) Average(ug/L)
Clinical Laboratory 15.4 35.5 21.7
Research  Laboratory 3 20.3 8.4
Incinerator 47.9 97.4 68.5
Laundry 4.3 43.5 20.6
Other 0.4 3.2 1.4

Table 2 - Typical Wastewater Composition by Facility Type - In HTML format

Table 2 - Typical Wastewater Composition by Facility Type - download as an Excel file.

The pilot system must not increase the concentration of any other regulated pollutants to levels greater than that allowed by the MWRA standards as are codified in Section 360 CMR 10.024, a copy of which is included as Attachment A. [Note: This section must be completed for the specific wastewater stream(s) to be included in the pilot test, and the entire RFP must be tailored specifically for your institution as noted in the cover letter accompanying this RFP. For technical assistance in how to modify this generic RFP into a site-specific document, you may wish to contact Bob Gingras, Vice President Wastewater Compliance Programs, EBI Consulting, 617-715-1816, bgingras@ebiconsultants.com.]

3.0 Scope of Work

The scope of work has been separated into activities that are the responsibility of the institution (client) and those that are the responsibility of the vendor.

For this pilot study, the client agrees to:

  • provide supervised access to the facility, as needed, to design and install the pilot test equipment.
  • provide access to electricity, potable water, process water, compressed air, and other common industrial utilities present at the facility during the time of this pilot test. Note: The vendor will be responsible for plumbing into the existing wastewater collection and discharge system(s) to obtain the side stream to be tested and for connecting into whichever of the other facility utility services as may be required to operate the pilot test equipment.
  • provide disposal of all aqueous process wastewater residuals from testing. For this project, aqueous residuals are limited to the wastewater being subjected to the pilot testing. Note: As specified in the vendor's responsibilities below, the vendor is responsible for disposal of all hazardous wastes, concentrated backflushing wastewaters (that may contain pollutants at concentrations in excess of MWRA discharge limits), excess treatment chemicals and any other chemical wastes generated by the pilot test system.
  • provide access to historical wastewater monitoring records.
  • conduct sampling and/or perform analysis of split/duplicate samples, provided by the vendor, at a Massachusetts certified contract analytical laboratory at the client's expense.

In the proposal responding to this RFP, bidders must:

  • provide a detailed description of pilot testing equipment for technical feasibility review, including the system type (resin-based, adsorption, electrolytic, etc.) and materials of construction (PVC, stainless steel, etc.). The pilot testing equipment must include, at a minimum, an equalization vessel providing 30 minutes retention time, a prefilter system, of specified rating, and sampling ports in the effluent line from each of the unit operations included in the system. See Figure 1 for an illustration of where sampling ports would be required for a conceptual system.
  • specify the utilities required for the pilot-scale pretreatment system.
  • provide a detailed breakdown of the fixed price cost that will be incurred by the client in bidder's completion of the in situ pilot trial as described herein.

Figure 1. Illustration of Process Sampling Requirements

Note: Five sampling points would be required for this treatment system. The number of process samples required to be taken will vary based upon the design of the treatment system. The vendor must estimate the number of samples to be analyzed to demonstrate attainment of steady-state based upon anticipated wastewater characteristics and ease of treatment system startup.

 
  • estimate the personnel and operating space requirements of the pilot-scale system.
  • estimate the residuals to be generated by the pilot-scale system, and specify how they will be managed.
  • specify the lead time required for delivery of the pilot test equipment.
  • include references from three recent clients that have used the same technology proposed for use in the pilot study.

Subsequent to award, the vendor must:

  • submit a draft pilot test workplan to the client for review and comment prior to equipment installation. This workplan must specify how the vendor proposes to remove the side stream to be tested from the facility piping. Following receipt of client's comments to the draft pilot test workplan, a final workplan must be submitted.
  • design, deliver, furnish and install all equipment, labor and appurtenances required to establish, to steady state operation over a period of 2 to 3 weeks, an in situ system designed for mercury removal. The system must be provided with sample ports designed to allow sampling following each of the unit operations (as indicated in Figure 1) to allow determination of serial mercury removal rates throughout the system.
  • plumb into the existing wastewater discharge line to obtain the side stream needed for the pilot testing.
  • conduct sampling as per 40 CFR 136 requirements and submit flow proportional samples taken over a complete process day to an EPA-approved and MA DEP certified laboratory for analysis. Grab samples should be obtained to analyze for pollutants that cannot be accurately analyzed from composite samples. EPA method 245.1 capable of achieving a method detection limit (MDL) of 0.2 ppb (g/L) must be used for mercury analysis (see Attachment B for method specifications). The vendor is expected to have and follow a standard quality assurance/quality control (QA/QC) procedure during this sampling. The QA/QC procedure may be either an EPA protocol or a vendor-developed procedure, if it meets EPA minimum requirements. One set of flow proportional day-long composite samples must be collected from each sampling port present in the system on each day for the last ten (10) days of the pilot test period following attainment of steady-state. These samples shall be subsequently analyzed by the vendor for mercury content (at a minimum). The client reserves the right to split a portion of each sample for his own analysis.

Subsequent to completion of field activities, the vendor must present his findings in a summary report which shall address each of the following issues in sufficient detail as may allow interpretation of the information by the client.

  • specify the utilities required for the full-scale treatment system.
  • prepare equipment lists and process schematics of the proposed full-scale treatment system.
  • summarize the data obtained during the pilot testing and estimate the capital, installation and O&M costs for a full-scale system. See Section 4.0 below.
  • estimate the spatial (envelope) requirements of the full-scale system.
  • estimate the residuals to be generated by the full-scale system.
  • conclude that the pilot test, as conducted, should be considered a success or provide recommended steps to improve the performance of the system tested. If the results indicate that the IWWT system tested is not likely to achieve the desired mercury concentrations, provide suggestions on how to enhance the existing equipment or suggest equipment to be used in place of the equipment tested.

4.0 Deliverables

As noted above in Section 3.0, the primary project deliverable will be the pilot test summary report. In this report, the vendor must provide: a succinct presentation and interpretation of the pilot test data; an estimate of the design and implementation (capital and installation) costs (+10 percent); and the expected performance of a full-size system. This report must include an appendix or attachment containing all raw mercury concentration data obtained during the pilot testing.

The report shall be of a format chosen by the vendor. The following format is suggested, as it may facilitate inclusion of all information required by this RFP:

1. Introduction/Background

2. Test Materials, Procedures, and Experimental Protocol

3. Pretreatment Considerations (including interferences)

4. Test Results (including total and dissolved removal rates for mercury and the 12 Priority Pollutant Metals)

5. Full Scale System Considerations (cost estimate for recommended full-scale treatment system to within +10 percent, O&M Requirements).

6. Discussion/Conclusions

7. Appendices (including detailed including information on reactor design information such as hydraulic retention time and loading rates, all analytical test results generated during the study, sampling QA/QC procedures followed, quantification and characterization of all residuals generated, and a summary of any operating and maintenance difficulties encountered during the pilot testing)

5.0 Cost and Schedule

Each bidder is required to include a firm (not-to-exceed) cost for this project and an anticipated schedule of execution based upon the information provided in this RFP. The not-to-exceed cost estimate must include allowances for the equipment, labor and appurtenances required to install and operate the system for a two week period after attaining steady state (2 to 3 weeks). The information contained in this RFP is expected to provide all of the information necessary to allow each bidder to prepare an accurate cost estimate and implementation schedule. However, the person specified in the cover letter accompanying this RFP may be contacted if clarifying information is required.

This RFP should specify the length of time required to initiate installation of the pilot test equipment after authorization to proceed has been received, along with an estimate of how long it will take the wastewater pretreatment system to attain steady state. Bidders should provide an estimate of the time that will be required to debug and reach steady-state operations.

Pilot test equipment must be removed within two weeks following completion of the ten (10) day effluent testing period. The Report, described in Section 4.0, must be submitted to the client no later than six weeks following completion of the pilot test.

 

Guidelines for the Preparation of a Request for Proposals for an In-Situ Pilot-Scale Feasibility Study of Mercury Removal Technology

 

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08/16/2006

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